Vacuum Pilot 110 Bottle Lab Freeze Dryer Lyophiliser

Brand Name:NANBEI
Certification:CE/ISO/SGS
Model Number:Vacuum freeze dryer
Minimum Order Quantity:1/set
Delivery Time:5-7days
Payment Terms:L/C, D/A, D/P, T/T, Western Union, MoneyGram
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Location: Zhengzhou Henan China
Address: No. 72, Beihuan Road, Jinshui District, Zhengzhou, Henan, China
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Product Details

Vacuum Freeze Dryer Vacuum Dryer Manufacturer Price Laboratory Vacuum Pilot Freeze Dryer Lyophilizer


Vacuum freeze dryer

Product features

1. High quality equipment and matching solutions were provided.Different system functions and components configuration can be customized in order to meet different users' needs.

2. The parts were compacted for the modular design, so the equipment was easy to maintain and operate.

3. The interface of the control system was friendly, the operation was convenient and the function was powerful.

4. It was highly close to the principles of production machines.

5. Configuration parts of well-known brands at home and abroad were used.

6. The treatment of parts surface is meeting or exceeding the relevant national or industry regulations.

7. AII interfaces shall be flange mounted.

8. All kinds of sensors were equipped.Timely alarm and active protection will be took when the function of the equipment were abnormal.

9. In order to easily operate in the clean room, external drying box can be connected for the small experimental freeze -drier.

10. Pilot freeze-drier was designed in accordance with the national pharmaceutical machinery industry standard.

Control system

The control system was composed of programmable logic controller, man-ma-chine interface device, sensor, terminal relay and digital to analog conversion module. The industrial intelligent control software was based on professional programmable controller and developed by advanced configuration configuration software for vacuum freeze-drying equipment.It was that can display the system status, process flow, alarm point and operation situation of each component, and can be monitored remotely.

1. It can automatically control the whole freeze-drying process with one key,and also can realize the freeze-drying process manually;

2. The system can show a variety of language interfaces such as Chinese and English [Russian, India (export optional)]. The system vacuum can be freely converted at mbar, Pa and Torr. The temperature can be expressed in degrees Celsius and Fahrenheit ;

3. During the operation, the system can automatically monitor and detect and record and store the relevant data. It can also be monitored by remote systems ;

4. From freeze-drying process to defrosting process, all materials can be programmed automatically and many programs can be stored ;

5. The system was equipped with variety sensors, it can alarm immediately during the operation of abnormal temperature or pressure, and take active protection to ensure safe and stable operation ;

6. Many data such as real-time-record of vacuum,cold trap temperature, material temperature, shelf temperature, operation error alarm were in this system ;

7. Data was recorded once a minute with freeze-drying curve. The system can record real-time data continuously and has USB data storage serial port ;

8. The freeze-drying process was recorded, the freeze-drying curve was drawn and the eutectic point test was achieved ;

9. The man-machine interface equipment of the control system can work stably in the environment from -20 to 65 degrees Celsius. It conforms to the NEMA (International Electric Manufacturing Association) protection regulations and the European CE Electrical Certification standards ;

10. Automatic vacuum regulation was achieved in this system.


Freeze-drying process

The freeze-drying cycle system consists of intermediate medium, circulating pump, heater,plate heat exchanger, freeze-drying chamber, shelf and pipeline. The freezing and heating of materials are completed with this system.

1. The freeze-drying process was managed. A number of mature and safe freeze-drying process were stored in the management system. Users can make up for different products of freeze-drying process when they adjusted freeze -drying process data;

2. Material can be observed and the freeze-drying parameters can be adjusted at any time in the freeze-drying process;

3. The freeze-drying chamber can effectively pre-freeze the material, and it is suitable for various serum bottles or vials;

4. PID algorithm is used in the automatic control. Materialscan be repeated freeze quickly or slowly;

5. The temperature was even by accurately controlling the medium circulating in the shelf heating system and the shelf was smooth with the special process. The quality of freeze drying and the drying efficiency were improved;

6. In order to avoid the contamination of the material after freeze drying, the protection system can be filled with pure nitrogen gas or other protective gas through the system;

7. The gland system can perform manual or automatic accurate and reliable sealing of the material container in the freeze-drying chamber in a vacuum state, the container lid and the container can be reliably sealed;

8. The ice condenser can be defrosted rapidly through the defrost system after freeze-drying process so as to freeze the material again.


Vacuum system

The system is composed of vacuum pump or roots pump (optional), freeze- drying box, vacuum gauge, pipeline and controller. The vacuum pump was equipped with redundancy.

1. The vacuum degree was controlled by PID mode, and the whole automatic control can be realized;

2. Systematically standardized test procedures were took in order to avoid potential vacuum leaks;

3. A device at the suction port of the vacuum pump was provided to prevent the gas flowing back when the equipment was stopped. An oil mist filtering device at the exhaust port is provided to prevent the exhaust gas polluting the surrounding environment;

4. The vacuum can be adjusted automatically or manually. The efficiency of the heat transfer and freeze drying was increased and the equipment and energy consumption was reduced;

5. The butterfly valve of the pilot freeze-drier between the freeze-drying chamber and the ice condenser should be closed before freeze-drying preparation and the terminative process. So the material can be handled and pre-frozen in a clean environment.


Refrigeration system

The utility model was composed of a refrigeration compressor, a condenser and an expander, etc. An imported compressor was adopted in the system. The shelf and the water catcher were respectively cooled by the slicon oill and the condensing pipe. The system was simple and reliable. The cold capacity was enough also.The environment-friendly refrigerant was used in the system. The system can be delay started and automatic controlled.


Selection Guide

Drying chamber device

1. Standard type: Suitable for bulk (powder, granule, solution) materials before freeze-drying.

  • Gland type: Suitable for freeze-dried materials filled into vials.
  • Multi-manifold type: Suitable for external bottled materials in eggplant-shaped bottles and jars, and freeze-drying multiple varieties at the same time.
  • Type T: Suitable for freeze-dried materials in ampoule tubes.

Optional accessories

1. Multi-manifold bottle hanging device, lyophilized bottle (eggplant-shaped bottle and jar), ampule tube lyophilized rack

2. Imported vacuum pump, high-speed vacuum pump oil, vacuum pump exhaust port oil mist filter, vacuum pump intake port dust filter

3. Ampoule tube sealer, Vial capping machine

4. Eutectic point tester, inert gas filling port

5. Stainless steel two-story experimental trolley

Technical Parameters

Experimental type Pilot typeProduction type
ModelUnit12A10C10E25C25E15E22E30E20G30G40G50E80E100E120E200300500
Effective partition aream20.120.10.250.150.220.30.20. 30.40.50.80.981.222.163.245.67
Water catching capacityKg23678152050605.67
22 mm vialbottle1101103903365046724486728709801450216027004800750013300
16 mm vialbottle2002007596389271276851124016501870280092001400025200
Partition size

mm

Φ180312x 242335 x 300300x 420320x500405x 605

600x

600

600x

900

900 x 900
(Length x width)Φ170®180Φ277
Available partitionspcs5423423445456+17+1
Interlayer spacingmm705045767014390651439065689010076100
Standard cold trap temperature-60 Ambient temperature≤30)-62 (Ambient temperature≤30)-80(Ambient temperature≤30)
Ultimate cold trap temperature≤-47-65(Ambient temperature≤25)-65(Ambient temperature≤25)-83 (Ambient temperature≤25)≤-70 (Ambient temperature≤30)
Standard vacuumPa5(no- load)5(no- load)5(no- load)10(no- load)10(no- load)
Ultimate vacuumPa1(no- load)1(no- load)1(no- load)1(no- load)≤10(no- load)
Shelf temperature rangeElectric heating(50)Electric heating(50)-50-+70-50-+70
Dimensions

mm

540 x 540 x 370

610x 610

x460

640x540x845

650x700x1288


700x800x

1550

1520x730x14001490x 780x 1710

2000 x 950x

1700

Length X Width X Height
Applicable power supplyAC220V 50HZAC380V 50HZ Three-phase five-wire system(OptionalAC220V 50HZ)AC380V 50HZ Three-phase five-wire system
Total powerW10001250140019002150330042008600180002100025000
WeightKg55851202502552602902953006507501300
Applicable environmentAmbient temperature≤30

Technical features list

Experimental type Pilot typeProduction type
Model12A10C10E25C25E15E22E30E20G30G40G50E80E100E120E200300500
Pre-freezing function
Partition silicone oil cooling and heating
Accurate temperature control of the partition
Controllable heating rate
Upgradable PLC control system
Color touch screen
Automatic control
Partition electric heating
Display freeze-drying curve and data
The upper computer monitors the lower computer
Wireless connection remote control
Large-capacity data storage
Cold trap automatic defrosting
Controllable vacuum
Capping system
Eutectic point test
CMP clean room installation
Air cooling
Multi-manifold device
T-frame for ampoules
Freeze-drying endpoint test
Circulating water cooling
Online disinfection
Online cleaning

●Indicates that it has the function ◑Indicates optional ○Indicates that the function is not applicable

China Vacuum Pilot 110 Bottle Lab Freeze Dryer Lyophiliser supplier

Vacuum Pilot 110 Bottle Lab Freeze Dryer Lyophiliser

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